Effect on environmental O2 on dynamical process of the Si(111)1~1-7~7 structual phase transition

Kazuyoshi Shimada, Satoshi Katsube, Tetsuya Ishimaru, Hiroki Kawada, and Iwao Ohdomari@

Surf. Sci. Vol.433-435, pp.460-464, 1999.


Abstract

Effect of environmental O2 on dynamical process of the Si(111)"1~1"¨7~7 structural phase transition has been investigated. In a macroscopic view, growth of the 7~7 DAS structure on the quenched surface after pulsed laser irradiation was monitored in-situ with RHEED under different O2 pressures. In an atomic scale view, the n~n DAS domain growth was observed with high temperature STM. It has been found that the oxides formed in the "1~1" matrix or phase boundary between n~n DAS-1~1 and the n~n domain boundary is responsible for the suppression of the 7~7 growth. Under the higher O2 pressure, not only suppression of the 7~7 growth but also erosion of the 7~7 took place. The threshold O2 pressure which suppresses the 7~7 domain growth but does not attack the 7~7 domains themselves was higher for the specimen kept at 600Ž than that at 465Ž because of the much less phase boundaries in the former.



The normalized (3/7,4/7) reflection intensity changes after laser irradiation on samples at 465 Ž (a) and at 600 Ž (b). The more the O2 pressure, the more the intensity increase was suppressed. Exposure to O2 is less effective at 600 Ž than 465 Ž.